D

Dumas Method

M = (ρ × V × 22,400) / (mass of gas at STP)
Quick Reference
Formula / NotationM = (ρ × V × 22,400) / (mass of gas at STP)
Also Known AsDumas bulb method, vapour density method, molar mass by vapour density

What is Dumas Method?

A classical analytical technique for determining the nitrogen content of organic compounds. The sample is burned in excess oxygen, and the resulting nitrogen gas is measured volumetrically. The method was developed by Jean-Baptiste Dumas in the 19th century.

Formula & Notation

M = (ρ × V × 22,400) / (mass of gas at STP)

Other Names / Synonyms: Dumas bulb method, vapour density method, molar mass by vapour density

Properties & Characteristics

The Dumas method is a classical technique for determining the molecular weight of a volatile liquid or gas. The substance is vaporised in a Dumas bulb (a sealed glass bulb) at a known temperature and pressure, and the volume of vapour is measured. Applying the ideal gas law (PV = nRT or the measured density compared to air), the molar mass is calculated. It was developed by Jean-Baptiste Dumas in the 19th century.

Uses & Applications

The Dumas method was historically used to determine molar masses of organic compounds and gases (chloroform, ethanol, benzene vapour). Modern alternatives include mass spectrometry and osmometry, but Dumas's principle is still taught in undergraduate chemistry and is used for simple gas density measurements.

Safety Information

The Dumas method requires heating glass bulbs to above the boiling point of the test liquid. Risk of glass bulb implosion or explosion if heated unevenly or if the substance has an unexpected vapour pressure. Use proper glass-handling precautions and protective screens if necessary.

Always consult the SDS/MSDS before handling any chemical. This information is for educational purposes only.

Key Facts

Term Dumas Method
Formula M = (ρ × V × 22,400) / (mass of gas at STP)
Synonyms Dumas bulb method, vapour density method, molar mass by vapour density

Frequently Asked Questions

A classical analytical technique for determining the nitrogen content of organic compounds. The sample is burned in excess oxygen, and the resulting nitrogen gas is measured volumetrically. The method was developed by Jean-Baptiste Dumas in the 19th century.

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