X

X-Ray Diffraction

Bragg's law: 2d sinθ = nλ; powder or single crystal XRD
Quick Reference
Formula / NotationBragg's law: 2d sinθ = nλ; powder or single crystal XRD
Also Known AsXRD, powder diffraction, Bragg diffraction, crystal diffraction

What is X-Ray Diffraction?

The scattering of X-rays by the regular array of atoms in a crystal, producing a characteristic diffraction pattern. Bragg's law (nλ = 2d sinθ) relates the wavelength, interplanar spacing, and diffraction angle. The pattern is used to determine crystal structure and identify compounds.

Formula & Notation

Bragg's law: 2d sinθ = nλ; powder or single crystal XRD

Other Names / Synonyms: XRD, powder diffraction, Bragg diffraction, crystal diffraction

Properties & Characteristics

X-ray diffraction (XRD) is an analytical technique that uses the diffraction of X-rays by crystalline materials to determine crystal structure, lattice parameters, and phase composition. In powder XRD, a fine-grained sample produces a diffraction pattern (diffractogram) characteristic of the crystalline phase. Each crystalline material has a unique diffraction fingerprint. The technique can identify phases and measure crystallite size via Scherrer equation.

Uses & Applications

Powder XRD is used in pharmaceuticals to identify polymorphic forms of drug substances, which affect solubility and bioavailability. It is used in geology and mineralogy to identify minerals. Materials science uses XRD to characterise new materials, thin films, and nanostructures.

Safety Information

XRD instruments use ionising X-radiation and must be properly shielded and interlocked. Operators must follow radiation safety protocols and undergo regular training. The instrument enclosure must not be opened while X-rays are generated.

Always consult the SDS/MSDS before handling any chemical. This information is for educational purposes only.

Key Facts

Term X-Ray Diffraction
Formula Bragg's law: 2d sinθ = nλ; powder or single crystal XRD
Synonyms XRD, powder diffraction, Bragg diffraction, crystal diffraction

Frequently Asked Questions

The scattering of X-rays by the regular array of atoms in a crystal, producing a characteristic diffraction pattern. Bragg's law (nλ = 2d sinθ) relates the wavelength, interplanar spacing, and diffraction angle. The pattern is used to determine crystal structure and identify compounds.

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